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SEM-Raman system

SEM-SCA at Bologna UniversityThe Renishaw structural and chemical analyser (SCA) unites two well-established technologies, scanning electron microscopy (SEM) and Raman spectroscopy, resulting in a powerful and unique technique which allows morphological, elemental, chemical, physical, and electronic analysis without moving the sample between instruments.

Application notes are available to download as PDF documents (registration required on download request).

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SCA Geological applications note - sandstone

[314KB]

 

The SEM-SCA is used to investigate a sandstone sample from the Loch Torridon area of NW Scotland, identifying the component minerals and their phases.

 

Image of sandstone from Loch Torridon

Capabilities

  • Morphology and mean atomic number
    from SEM (SEI and BEI)
  • Elemental composition
    from EDS analysis
  • Chemical composition and identification
    from Raman spectroscopy
  • Physical structure
    (crystallographic and mechanical data) from Raman spectroscopy
  • Electronic and physical structure
    from CL and PL spectroscopies

Applications

These include:

  • Materials science
    corrosion studies, electronic materials, polymers, composites
  • Semiconductors
    particle contamination identification
  • Pharmaceuticals
    coating, filler and excipient identification, polymorphism studies
  • Forensic science
    identification of explosives, drugs, fibres, pigments

Advantages

  • Simultaneous SEM and Raman spectroscopy
    Features of interest can be easily located using the SEM. These can then be identified rapidly and unambiguously using Raman spectroscopy.
  • EDS and white light images from the same sample position
    EDS spectra, maps, and white light images can be acquired from the same sample position as the SEM image and the Raman spectra.
  • Cathodoluminescence (CL) and photoluminescence (PL) spectroscopies
    The Raman collection optics are fully compatible with both PL and CL spectroscopies. The former uses a laser as the excitation source, the latter the electron beam. Each technique can reveal both electronic and physical information about the sample, and CL can be sensitive to very subtle changes in composition and residual strain.

Overview of SEM-Raman system

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Renishaw's structural and chemical analyser (SCA) for scanning electron microscopes

[454KB]

 

Renishaw's structural and chemical analyser enhances scanning electron microscopes by adding the chemical analysis powers of Raman spectroscopy (four page brochure)

 

Applications

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SCA geological application note - heavy mineral sands

[494KB]

 

Combined SEM and Raman analysis of heavy mineral deposits from South Africa. These deposits are a valuable source of titanium, zirconium, and iron.

 

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SCA geological application note - meteor and clinker

[410KB]

 

Using the SEM-SCA to analyse Portland cement clinker and meteorites (four pages).

 

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SCA oxidation application note - cultural heritage

[354KB]

 

SEM-SCA analysis helps in the preservation of a corroding bronze statue of the Greek god Ares from the ancient city of Zeugma in Turkey.

 

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SCA oxidation application note - copper and steel

[345KB]

 

This note illustrates how the SEM-SCA can be used to study the corrosion of copper wire and nuclear reactor steel (four pages).

 

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SCA Geological applications note - sandstone

[314KB]

 

The SEM-SCA is used to investigate a sandstone sample from the Loch Torridon area of NW Scotland, identifying the component minerals and their phases.

 

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A SEM-SCA study of single-wall nanotubes

[76KB]

 

A study of single-wall nanotubes using Renishaw's structural and chemical analyser for scanning electron microscopes

 

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Combined SEM and optical spectroscopy: new tools for characterising materials

[808KB]

 

One page flyer illustrating the use of Renishaw's SEM-SCA to characterise materials, using results from a diamond film as examples.

 

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Structural and chemical analyser for SEM

[705KB]

 

One page flyer illustrating the use of the SEM-SCA for analysing cemented diamond composites.

 

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Analysing carbon nanotubes with Renishaw's SCA

[593KB]

 

One page flyer with carbon nanotube spectra.

 

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Classifying meteorites using Renishaw's structural and chemical analyser

[1.9MB]

 

One page flyer describing the use of SEM imaging and Raman spectroscopy in studies of meteorites.

 

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Characterisation of particulates on semiconductors using the SEM-SCA

[240KB]

 

The SEM-SCA identifies particulate contaminants on semiconductors as polymers and polishing materials (four pages).

 

Next steps

Contact us online if you require more information or you have a pricing query, or alternatively you may like to speak directly to your local Renishaw office.